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In the last few years, many efforts have been spent inthe analytical chemistry area for developing methodologieswith suitable productivity and sensitivity, especially inthe water analysis field. In this context, FIA systems havebeen successfully coupled to solid-phase extraction (SPE)for the preconcentration/separation of metallic cations withseveral types of no modified solid sorbents, such as C18 [1]polyurethane foam [2–5], activated carbon [6], activated alumina[7, 8] or fullerene [9].
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