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(1) Calibration of the electrode:a. Calibration of electrode potential must be done each days or before analysis of sample bath.b. Prepare four calibration standards using 100-mL volumetric flasks as follows:- Standard A - 5.00 mL of sodium sulfide stock solution, 50 mL of SAOB and dilute to a total volume of 100 mL with water.- Standard B - 1.00 mL of sodium sulfide stock solution, 50 mL of SAOB and dilute to a total volume of 100 mL with water.- Standard C - 2.00 mL of calibration standard A, 50 mL of SAOB and dilute to a total volume of 100 mL with water.
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